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12901 Inorganic Chemistry Laboratory II - Five-year degree in Chemistry


Center
Faculty of Chemistry
Departament
Inorganic Chemistry
Lecturers in charge
Sin datos cargados
Met. Docent
Individual and group work.
Met. Avaluació
Final examination and project work
Bibliografia
Cuadernillo de prácticas.
Continguts
GENERAL OBJECTIVES

During the practicals included in this course the student
approaches preparative chemisty, the study of properties and characterization
of particles in aqueous breakup of diverse compounds.
.The study is centered on some of the more significant elements
of the first cycle. The use of different
physical techniques of characterization (visible and infrared spectoscopes,
measure of magnetic susceptibilities, measures of
conductivity, polarimetry etc.) together with the analysis and
interpretation of the obtained data is also part of the student's training
in their second cycle with of Inorganic Laboratory Chemistry.

Content:

BLOCK I
- Co(III) Complexes (four sessions).
BLOCK II
- Synthesis of Ni(II) compounds of the formulae [Ni(NO2)2(NH3)4] and
KNiF3 (a session).
- Preparation of the oxalate compounds of the formulae [Fe(C2O4)2(H2O)2] and
K3[Fe(C2O4)3]. 3H2O (a session).
- The experimental study from diagrams of levels of energy of d8 ion in the
field of octahedron ligands (a session).
- Experimental measure of the magnetic moment of four iron complexes of the formulae
K3[Fe(C2O4)3]. 3H2O, K3[Fe(CN)6], [Fe(C2O4)2(H2O) 2] and K4[Fe(CN)6] (a session).
BLOCK III
- Preparation and measure of the magnetic moment of the hexa-fluourophosphate
[Fe(h5-C5H5)2]PF6 (a session).
- Prepar